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Put the flask as part of your freezer for approximately ½ hour or right up until temp drops to 5 deg C. Pour the answer right into a pyrex dish and slowly and gradually evaporate about small heat. Never evaporate wholly. Upcoming, area the solution again with your washed Erlenmeyer and include about 275 ml dH2O. It should dissolve a little bit. Magnetically stir and start heating the solution. Increase 172 ml of 2M HCl and keep on stirring and heating until eventually just boiling. At about 50-60 deg C the white Alternative need to change very clear all over again. Reflux all over again for around two.five hours magnetically stirring The complete time. Let to cool to home temp. White powder will look.
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